HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20263942, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20264049 | HCID 20264049 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20263942 | HCID 20263942 | — |
Reaction Steps
To a solution of 0.1 mole of 3-benzyloxy-4-hydroxymethyl-2-methyl-5-vinylpyridine in 500 ml. of benzene is added dropwise with cooling a solution of 0.11 mole of thionyl chloride in 50 ml. benzene. The reaction mixture is stirred for 1 hour and then filtered to give 2-methyl-3-benzyloxy-4-chloromethyl-5-vinylpyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061759 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-b9a33e92ff704113892c0e334532b604 |
| Source note | uspto-grants-1977_12 |