HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(4-methoxyphenyl)-2-methylprop-2-enoate → Ethyl 3-(4-methoxyphenyl)-2-methylpropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(4-methoxyphenyl)-2-methylprop-2-enoate | HCID 53711494 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(4-methoxyphenyl)-2-methylpropanoate | HCID 11160380 | — |
Reaction Steps
Ethyl p-methoxy-α-methylcinnamate (39.1 g) is dissolved in 186 ml of 2B ethanol. This solution is shaken with 1.5 g of 10% palladium on carbon at an initial pressure of 60 psi until the uptake of hydrogen is 100%. The reaction mixture is removed on an evaporator leaving ethyl β-(p-methoxyphenyl)-α-methylpropionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061771 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-821d54285fdb469ca550f9f116afb50e |
| Source note | uspto-grants-1977_12 |