huagongshe.com
HRID461117

反应详情

EQUATION

反应方程式

HRID 461117 的结构方程式

REACTANTS

反应物

2
结构：CCCCNC(=S)NCCCC
HCID2723622

N,N'-Dibutylthiourea

C9H20N2S

结构：NS(=O)(=O)c1cc(C(=O)CBr)ccc1Cl
HCID12952390

未命名化合物

PRODUCTS

生成物

1
结构：Br.CCCCN=C1SCC(O)(c2ccc(Cl)c(S(N)(=O)=O)c2)N1CCCC
HCID22760686

未命名化合物

PROCEDURE

实验过程

6.2 g of 2 bromo-4'-chloro-3'-sulfamoylacetophenone were reacted with 3.8 g of 1,3-di-n-butylthiourea according to the prescription given in Example 12 and the end product was precipitated with diisopropyl ether.

WORKUP

后处理

  1. customthe end product was precipitated with diisopropyl ether