1,3-(Dihexyl)thiourea → HCID 22760537, compound

HRID 461125Notes

Reaction equation

HRID 461125 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:22][C:23]([NH:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])=[S:24])[CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>>[ClH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:24][C:23](=[N:22][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[N:25]2[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31])=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 28012081,3-(Dihexyl)thioureaHCID 213167492,4'-Dichloro-3'-sulfamoylacetophenone

Product 1

HCID 22760537HCID 22760537, compound

Procedure

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane.

Workup

  1. customthe end product was precipitated with diethyl ether
  2. additionthe remaining oil was treated with cyclohexane

Sources & evidence

ORD record
ord-77fdb60e627d4fc88fbb36aa9fba915f
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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