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HRID461125

反应详情

EQUATION

反应方程式

HRID 461125 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCNC(=S)NCCCCCC
HCID2801208

1,3-(Dihexyl)thiourea

C13H28N2S

结构：NS(=O)(=O)c1cc(C(=O)CCl)ccc1Cl
HCID21316749

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCN=C1SCC(O)(c2ccc(Cl)c(S(N)(=O)=O)c2)N1CCCCCC.Cl
HCID22760537

未命名化合物

PROCEDURE

实验过程

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-di-n-hexyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diethyl ether and the remaining oil was treated with cyclohexane.

WORKUP

后处理

  1. customthe end product was precipitated with diethyl ether
  2. additionthe remaining oil was treated with cyclohexane