Thiourea, N,N'-di-2-propen-1-yl- → HCID 22760653, compound

HRID 461126Notes

Reaction equation

HRID 461126 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:19][C:20]([NH:22][CH2:23][CH:24]=[CH2:25])=[S:21])[CH:17]=[CH2:18]>>[ClH:1].[CH2:23]([N:22]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:19][CH2:16][CH:17]=[CH2:18])[CH:24]=[CH2:25]

Participants

3

Reactant 2

HCID 3034186Thiourea, N,N'-di-2-propen-1-yl-HCID 213167492,4'-Dichloro-3'-sulfamoylacetophenone

Product 1

HCID 22760653HCID 22760653, compound

Procedure

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 2.5 g of 1,3-diallyl-thiourea were reacted according to the prescription given in Example 12, the end product was precipitated with diisopropyl ether and the oil obtained was crystallized with diethyl ether/ethyl acetate (1:1).

Workup

  1. customthe end product was precipitated with diisopropyl ether
  2. customthe oil obtained
  3. customwas crystallized with diethyl ether/ethyl acetate (1:1)

Sources & evidence

ORD record
ord-5cc8fe9332a247b5ae3e0debc08538ed
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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