Bromo-4'-chloro-3'-sulfamoylacetophenone → HCID 21395273, compound

HRID 461127Notes

Reaction equation

HRID 461127 reaction equation
[Br:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH2:16]([NH:19][C:20]([NH:22][CH:23]([CH3:25])[CH3:24])=[S:21])[CH:17]=[CH2:18]>>[BrH:1].[CH2:16]([N:19]1[C:3]([C:5]2[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=2)([OH:4])[CH2:2][S:21][C:20]1=[N:22][CH:23]([CH3:25])[CH3:24])[CH:17]=[CH2:18]

Participants

3

Reactant 2

HCID 12952390Bromo-4'-chloro-3'-sulfamoylacetophenoneHCID 19650614HCID 19650614, compound

Product 1

HCID 21395273HCID 21395273, compound

Procedure

6.2 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 3.16 g of 1-allyl-3-isopropylthiourea were reacted according to the prescription given in Example 23 and the colorless crystalline end product was filtered off.

Workup

  1. filtrationthe colorless crystalline end product was filtered off

Sources & evidence

ORD record
ord-0afbd0d69233479baebc35b7da48a143
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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