N,N'-Dicyclopropylthiourea → 59814-71-0

HRID 461133Notes

Reaction equation

HRID 461133 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]1([NH:19][C:20]([NH:22][CH:23]2[CH2:25][CH2:24]2)=[S:21])[CH2:18][CH2:17]1>>[ClH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:21][C:20](=[N:19][CH:16]3[CH2:18][CH2:17]3)[N:22]2[CH:23]2[CH2:25][CH2:24]2)=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 17750075N,N'-DicyclopropylthioureaHCID 213167492,4'-Dichloro-3'-sulfamoylacetophenone

Product 1

HCID 2276056759814-71-0

Procedure

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 3.1 g of 1,3-dicyclopropylthiourea were reacted according to the prescription given in Example 12 and the colorless crystalline precipitate of the end product was filtered off.

Workup

  1. filtrationthe colorless crystalline precipitate of the end product was filtered off

Sources & evidence

ORD record
ord-3126803682484742bbee70a79c7d8345
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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