Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylthiourea → 4-(4-Chloro-3-sulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol-hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylthiourea | HCID 727200 | — |
| 반응물 | 2,4'-Dichloro-3'-sulfamoylacetophenone | HCID 21316749 | — |
| 생성물 | 4-(4-Chloro-3-sulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol-hydrochloride | HCID 22760523 | — |
반응 단계
5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 4.8 g of 1,3-dicyclohexylthiourea were reacted according to the prescription made in Example 12, the end product was precipitated with 200 ml of diethyl ether and the oil was crystallized after decanting the solvent with diethyl ether. Colorless, crystalline solid body: melting point: 177° C (from acrylonitrile).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04061761 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-0cba33b3992a44f6a9575dbd8486e604 |
| 출처 메모 | uspto-grants-1977_12 |