2,4'-Dichloro-3'-sulfamoylacetophenone → HCID 22760581, compound

HRID 461135Notes

Reaction equation

HRID 461135 reaction equation
[Cl:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([Cl:11])=[C:7]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:6]=1)=[O:4].[CH:16]1([NH:24][C:25]([NH:27][CH:28]2[CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]2)=[S:26])[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1>>[ClH:1].[Cl:11][C:8]1[CH:9]=[CH:10][C:5]([C:3]2([OH:4])[CH2:2][S:26][C:25](=[N:24][CH:16]3[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]3)[N:27]2[CH:28]2[CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]2)=[CH:6][C:7]=1[S:12](=[O:15])(=[O:14])[NH2:13]

Participants

3

Reactant 2

HCID 213167492,4'-Dichloro-3'-sulfamoylacetophenoneHCID 22760561HCID 22760561, compound

Product 1

HCID 22760581HCID 22760581, compound

Procedure

5.2 g of 2,4'-dichloro-3'-sulfamoylacetophenone and 5.8 g of 1,3-dicyclooctylthiourea were reacted according to the prescription made in Example 12 and worked up according to the prescription of Example 42. Colorless solid body, decomposition beginning at 118° C, γC=N 1600 cm-1.

Workup

  1. customat 118° C

Sources & evidence

ORD record
ord-37258eba47f84792afba17b3d34674ad
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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