HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-cyclohexyl-3-(pyridin-3-ylmethyl)thiourea → HCID 22760631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-cyclohexyl-3-(pyridin-3-ylmethyl)thiourea | HCID 4584896 | — |
| Reactant | Bromo-4'-chloro-3'-sulfamoylacetophenone | HCID 12952390 | — |
| Product | HCID 22760631 | HCID 22760631 | — |
Reaction Steps
4.7 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 3.7 g of 1-cyclohexyl-3-(3-pyridylmethyl)-thiourea were reacted as prescribed in Example 23. The end product precipitated first as oil and crystallized after stirring for several hours at room temperature. Colorless crystals, melting point 140° C, decomposition beginning at 165° C, γC=N 1600 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-b6ea30725203430fb168eff735a7ac67 |
| Source note | uspto-grants-1977_12 |