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HRID461152

反应详情

EQUATION

反应方程式

HRID 461152 的结构方程式

REACTANTS

反应物

2
结构：CCNC(=S)NCC
HCID2735009

N,N'-Diethylthiourea

C5H12N2S

结构：NS(=O)(=O)c1cc(C(=O)CCl)ccc1Br
HCID22760605

2-Bromo-5-(2-chloroacetyl)benzenesulfonamide

C8H7BrClNO3S

PRODUCTS

生成物

1
结构：CCN=C1SCC(O)(c2ccc(Br)c(S(N)(=O)=O)c2)N1CC.Cl
HCID22760569

未命名化合物

PROCEDURE

实验过程

4.6 g of 4'-bromo-3'-sulfamoyl-2-chloroacetophenone and 1.8 g of ground 1,3-diethylthiourea were reacted and worked up according to the prescription given in Example 12. Colorless solid body, decomposition beginning at 103° C, C=N 1615 cm-1.

WORKUP

后处理

  1. customat 103° C