HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → 3'-Sulfamoyl-diazoacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3'-Sulfamoyl-diazoacetophenone | HCID 53705814 | — |
Reaction Steps
11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-29a7aeba45ad449fbac66113ff177cd3 |
| Source note | uspto-grants-1977_12 |