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HRID461165

反应详情

EQUATION

反应方程式

HRID 461165 的结构方程式

REACTANTS

反应物

2
结构：CNC(=S)NC
HCID2723631

N,N'-Dimethylthiourea

C3H8N2S

结构：NS(=O)(=O)c1cccc(C(=O)CCl)c1
HCID22007172

未命名化合物

PRODUCTS

生成物

1
结构：CN=C1SCC(O)(c2cccc(S(N)(=O)=O)c2)N1C.Cl
HCID22760516

未命名化合物

PROCEDURE

实验过程

3.5 g of 2-chloro-3'-sulfamoylacetophenone and 1.56 g of ground 1,3-dimethylthiourea were reacted as prescribed in Example 12 and the end product was precipitated with a mixture of 1 part of diethyl ether and 2 parts of ethyl acetate. Colorless crystals, melting point: 184° C.

WORKUP

后处理

  1. customthe end product was precipitated with a mixture of 1 part of diethyl ether and 2 parts of ethyl acetate