HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylthiourea → HCID 22760533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylthiourea | HCID 2723631 | — |
| Reactant | HCID 22760520 | HCID 22760520 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22760533 | HCID 22760533 | — |
Reaction Steps
5.2 g of 2,4'-dichloro-3'-cyclooctylsulfamoylacetophenone and 1.8 g of 1,3-dimethylthiourea were reacted as prescribed in Example 23. To the reaction mixture were added 30 ml of ethyl acetate and the end product was filtered off. Colorless crystals, melting point: 192° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5e51b68b67614f37a75fb4693d2442db |
| Source note | uspto-grants-1977_12 |