Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 5-Acetyl-2-chlorobenzene-1-sulfonyl chloride | HCID 12619795 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22760438 | HCID 22760438 | — |
Reaction Steps
To a stirred mixture of 10 ml of 40% dimethyl amine solution and 60 ml of methanol, there were added, portionswise, 5.1 g of 4'-chloro-3'-chlorosulfonylacetophenone, so that the reaction temperature did not exceed 30° C. The reaction mixture was stirred for 3 hours at room temperature and 15 minutes at 60° C. After cooling, the reaction mixture was poured into 200 ml of water and the crystals were filtered off. Melting point: 108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04061761 |
|---|
| Source dataset | uspto-grants-1977_12 |
|---|
| ORD ID | ord-ab96505f96444dcd888e4ac1b02ab2e3 |
|---|
| Source note | uspto-grants-1977_12 |
|---|
