HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Diethylthiourea → HCID 22760425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Diethylthiourea | HCID 2735009 | — |
| Reactant | 2-Bromo-4'-chloro-3'-dimethylsulfamoylacetophenone | HCID 20476846 | — |
| Product | HCID 22760425 | HCID 22760425 | — |
Reaction Steps
6.8 g of 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 2.7 g of 1,3-diethylthiourea were reacted as prescribed in Example 23. The solvent was decanted and the oily precipitate of the end product was crystallized under fresh acetone. Colorless solid body, decomposition beginning at 154° C, γ C=N 1610 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-af832e3022c84cf68a3bd2bca7595ba7 |
| Source note | uspto-grants-1977_12 |