HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 22760637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 22760443 | HCID 22760443 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22760637 | HCID 22760637 | — |
Reaction Steps
2.5 g of 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-cyclohexyl-2-cyclohexylimino-1,3-thiazolidine-4-ol were dissolved in 10 ml of methanol and adjusted to pH 3 by adding dropwise 48% hydrobromic acid. The solvent was distilled off under reduced pressure and the amorphous end product was crystallized under diethyl ether. Colorless crystals, melting point: 131° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-96f5498b4c2d4450b2c7988010546d80 |
| Source note | uspto-grants-1977_12 |