HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22760593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 59210-68-3 | HCID 767898 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 22760593 | HCID 22760593 | — |
Reaction Steps
39 g of 4-chloro-3-diethylsulfamoylbenzoic acid were boiled under reflux in 200 ml of thionyl chloride until the development of HCl had finished and the thionyl chloride was then distilled off under reduced pressure. 4-chloro-3-diethylsulfamoylbenzoyl chloride was obtained as fair yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-aea846709bf7474ba820c7a21d8306bf |
| Source note | uspto-grants-1977_12 |