HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl N,N'-(oxydi-p-phenylene)dioxamate → HCID 21315031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl N,N'-(oxydi-p-phenylene)dioxamate | HCID 12264875 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21315031 | HCID 21315031 | — |
Reaction Steps
Diethyl N,N'-(oxydi-p-phenylene)dioxamate (2.0 gm.) is stirred at room temperature for 3 hours in 1.0 N sodium hydroxide (50 ml.). The solid is collected by filtration and dissolved in water. The pH is adjusted to pH=3 with concentrated hydrochloric acid and the desired product collected by filtration (1.6 gm., mp > 320°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061791 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5bc83309b9bf4ba6936602f8f80b3cb5 |
| Source note | uspto-grants-1977_12 |