HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 2-Mesyloxy-1,2,3,4-tetrahydro-tribenzo(b,d,f)-oxepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 22760978 | HCID 22760978 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Mesyloxy-1,2,3,4-tetrahydro-tribenzo(b,d,f)-oxepine | HCID 22760919 | — |
Reaction Conditions
| Temperature | 0 °C |
|---|
Reaction Steps
6.2 g of 2-hydroxy-1,2,3,4-tetrahydro-tribenzo(b,d,f)-oxepine are added to a mixture of 16.8 ml of pyridine and methane sulphonylchloride, after which the mixture is stirred for 2 hours at 0° C and then another 2 hours at room temperature. After that the mixture is poured out into water and then extracted with ether. The ether layers are dried and evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062840 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5d9a7db916b5465aa9a76f7826523b12 |
| Source note | uspto-grants-1977_12 |