HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 54335978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 22760937 | HCID 22760937 | — |
| Product | HCID 54335978 | HCID 54335978 | — |
Reaction Steps
1 g of 2-keto-1,2,3,4-tetrahydro-tribenzo(b,d,f)-oxepine is mixed with 1 ml of benzene, 15 ml of acetonitril and 0.5 g of molecular sieve (4 A). 50 mg of sodium-ethoxide are added and the mixture is heated for 3 hours (90°-100° C). After cooling the mixture the molecular sieve is filtered off and the filtrate evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062840 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-0469c27b78844eb09cd34f10f179ee17 |
| Source note | uspto-grants-1977_12 |