huagongshe.com
HRID46136

反应详情

EQUATION

反应方程式

HRID 46136 的结构方程式

REACTANTS

反应物

2
结构：CC1(CC2CCNCC2)SC(N[C@H]2CC3CCC2C3)=NC1=O
HCID178422083

未命名化合物

结构：CC(C)(C)OC(=O)NCCOc1cccc(C(=O)N2CCC(CC3(C)SC(N[C@H]4CC5CCC4C5)=NC3=O)CC2)c1
HCID178453727

未命名化合物

PRODUCTS

生成物

1
结构：CC1(CC2CCN(C(=O)c3cccc(OCCN)c3)CC2)SC(N[C@H]2CC3CCC2C3)=NC1=O
HCID178422098

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in the preparation of 2-((2S)-bicyclo[2.2.1]heptan-2-ylamino)-5-methyl-5-(piperidin-4-ylmethyl)thiazol-4(5H)-one by using tert-butyl 2-(3-(4-((2-((2S)-bicyclo[2.2.1]heptan-2-ylamino)-5-methyl-4-oxo-4,5-dihydrothiazol-5-yl)methyl)piperidine-1-carbonyl)phenoxy)ethylcarbamate (689 mg, 1.18 mmol) as the starting material. The title compound was obtained as an off-white solid (531 mg). MS (ESI, pos. ion) m/z: 485 (M+H)

WORKUP

后处理

  1. customThe title compound was prepared