HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → N-Butyl-11-(butylimino)-1-ethyl-1,5,6,11-tetrahydrobenzo-[5,6]cyclohepta[1,2-b]pyrazolo[4,3-e]pyridin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 4-chloro-1-ethyl-5,6-dihydrobenzo[5,6]-cyclohepta[1,2-b]pyrazolo[4,3-e]pyridin-11(1H)-one | HCID 20382073 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-Butyl-11-(butylimino)-1-ethyl-1,5,6,11-tetrahydrobenzo-[5,6]cyclohepta[1,2-b]pyrazolo[4,3-e]pyridin-4-amine | HCID 22757739 | — |
Reaction Steps
10.8 g. of 4-chloro-1-ethyl-5,6-dihydrobenzo[5,6]-cyclohepta[1,2-b]pyrazolo[4,3-e]pyridin-11(1H)-one (0.035 mol.) and 100 ml. of butylamine are reacted in an autoclave by the procedure of Example 5, yield: 9.8 g. (70%); m.p. 124°-125° (ether; refrigerator).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062858 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-05969edfc9004a38b70db3e29b7c3090 |
| Source note | uspto-grants-1977_12 |