HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propiolic Acid → HCID 45785051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propiolic Acid | HCID 10110 | — |
| Reactant | 2-(4-Chlorophenyl)-2-propynoic acid | HCID 18607 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 45785051 | HCID 45785051 | 54.1% |
Reaction Steps
p-Chlorophenylpropiolic acid (3.3 g) and propiolic acid (7.6 g) in acetic anhydride (80 ml) were refluxed for 12 hr. The solution was concentrated (to 40 ml) and the precipitate which formed on cooling was recrystallised from acetone to give 6-chloro-2,3-naphthalenedicarboxylic anhydride (2.3 g) m.p. 220°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062955 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-bc5c5b77306f4b05b1d17cab8e1b4fa9 |
| Source note | uspto-grants-1977_12 |