HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 44658157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 2,3-Bis(bromomethyl)naphthalene | HCID 262259 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 44658157 | HCID 44658157 | — |
Reaction Steps
An ethanolic diethylamine solution (100 ml) was added dropwise to 2,3-bis(bromomethyl)naphthalene (20 g) in ethanol (10 ml) kept at 0°. The precipitate which formed was filtered and recrystallised from propan-2-ol/water to give 2,2-diethylbenz[f]isoindolinium bromide m.p. 228°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062955 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-69fc5283a87d4f1289105e70457ca42b |
| Source note | uspto-grants-1977_12 |