1-Bromododecane → HCID 21393913, compound

HRID 461457Notes

Reaction equation

HRID 461457 reaction equation
[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]=[C:14]1[CH2:18][CH3:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:20]([Br:32])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31]>C(O)C>[Br-:32].[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]([CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH3:20])[CH:14]1[CH2:18][CH3:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 89191-BromododecaneHCID 13985530HCID 13985530, compound

Product 1

HCID 21393913HCID 21393913, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

0.38 mole of 1-n-dodecyl-2-ethylimidazole and 0.42 mole of n-dodecyl bromide are dissolved in 250 ml of ethanol and boiled with reflux for 5 hours. The solvent then is separated and the residue is washed with ether.

Workup

  1. temperaturewith reflux for 5 hours
  2. customThe solvent then is separated
  3. washthe residue is washed with ether

Sources & evidence

ORD record
ord-8016fbfb1cf74f5ab992598d37d2c59b
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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