1-Butanol → HCID 86735279, compound

HRID 461458Notes

Reaction equation

HRID 461458 reaction equation
C([C:13]1[N:14]=[C:15]([CH2:18][CH3:19])[NH:16][CH:17]=1)CCCCCCCCCCC.[CH2:20]([Cl:28])[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27].[CH2:29](O)[CH2:30][CH2:31][CH3:32]>>[Cl-:28].[CH2:27]([N:14]1[CH:13]=[CH:17][N:16]([CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[CH:15]1[CH2:18][CH3:19])[CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:29][CH2:30][CH2:31][CH3:32]

Participants

4

Reactant 3

HCID 2631-ButanolHCID 81421-ChlorooctaneHCID 178442819HCID 178442819, compound

Product 1

HCID 86735279HCID 86735279, compound

Conditions

Temperature
127 °C

Procedure

1 mole of n-dodecyl-2-ethylimidazole is dissolved in 500 ml of n-butanol and reacted with 1.2 moles of n-octyl chloride. This reaction mixture is heated at 127° C for 15 hours. Then the alcohol and the excess n-octyl chloride are distilled off and the remaining residue is washed with ether. Yield: 204 grams

Workup

  1. distillationThen the alcohol and the excess n-octyl chloride are distilled off
  2. washthe remaining residue is washed with ether

Sources & evidence

ORD record
ord-2a6b47ed5144480a8462c0b476ab4a41
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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