HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 86735283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | HCID 85931842 | HCID 85931842 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Product | HCID 86735283 | HCID 86735283 | — |
Reaction Steps
To a solution of 17.9 g of 3,3-dimethyl-2-oximinobenzodioxane and 5 drops of triethylamine was added 18.0 ml of methyl isocyanate. The reaction mixture was then left at ambient temperature for 16 hours. The reaction mixture was concentrated and filtered to yield 3,3-dimethyl-2-[O-(methylcarbamoyl)oximino]benzodioxane, m.p. 174°-176° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062969 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-bb3ad90ba25546838e27c7dff3b4b0b0 |
| Source note | uspto-grants-1977_12 |