Ammonia → Ethenesulfonamide, 2,2-diphenyl-

HRID 461473Notes

Reaction equation

HRID 461473 reaction equation
[C:1]1([C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[S:15](Cl)(Cl)(=[O:17])=[O:16].[NH3:20]>>[C:1]1([C:7]([C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=2)=[CH:8][S:15]([NH2:20])(=[O:17])=[O:16])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 222AmmoniaHCID 107401,1-DiphenylethyleneHCID 24648Sulfuryl chloride

Product 1

HCID 12218143Ethenesulfonamide, 2,2-diphenyl-

Procedure

When 1,1-diphenylethene reacts with sulfuryl chloride in N,N-dimethylformaide, followed by treatment with ammonia, according to the procedure of Preparation A, there is obtained 2,2-diphenylethenesulfonamide, m.p. 134°-135° C.

Workup

  1. customaccording to the procedure of Preparation A

Sources & evidence

ORD record
ord-23bf5005b9bc41d097e5705e513722e6
Source dataset
uspto-grants-1977_12
Patent number
US04062960

Reaction notes

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