2-Chloro-4-(1-chloroethyl)-1-cyclohexylbenzene → alpha-Methyl-para-cyclohexyl-benzyl chloride

HRID 461509Notes

Reaction equation

HRID 461509 reaction equation
Cl[C:2]1[CH:3]=[C:4]([CH:14]([Cl:16])[CH3:15])[CH:5]=[CH:6][C:7]=1[CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>C1CCCCC1.C(OCC)(=O)C>[CH:8]1([C:7]2[CH:2]=[CH:3][C:4]([CH:14]([Cl:16])[CH3:15])=[CH:5][CH:6]=2)[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13]1

Participants

3

Reactant 1

HCID 213939512-Chloro-4-(1-chloroethyl)-1-cyclohexylbenzene

Product 1

HCID 11806290alpha-Methyl-para-cyclohexyl-benzyl chloride

Reagents, catalysts & solvents 1

HCID 21867204Cyclohexane ethylacetateSolvent

Procedure

1-(3'-Chloro-4'-cyclohexyl-phenyl)-1-chloro-ethane, an oil, Rf -value 0.8 on carrier A with cyclohexane/ethyl acetate =4/1.

Sources & evidence

ORD record
ord-185c9f25e7aa4264bb871096795ca0e5
Source dataset
uspto-grants-1977_12
Patent number
US04062973

Reaction notes

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