HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 23037434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-((4-Methyl-5-imidazolyl)methylthio)ethylthiourea | HCID 12718697 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23037434 | HCID 23037434 | 62.1% |
Reaction Steps
a solution of N-[2-((5-methyl-4-imidazoly)methylthio) ethyl]thiourea (2.29g) and methyl iodide (1.56 g) in methanol (5 ml) was kept at room temperature for 18 hours affording S-methyl-N-[2-((5-methyl-4-imidazolyl)methylthio)ethyl]thiouronium iodide (2.3 g), m.p. 128°-131°. The iodide was converted into the corresponding sulphate by ion-exchange on an ion-exchange resin (IRA 401) in the sulphate form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062967 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-efa37a4a6e6141ed8ac0f544c84fa3e7 |
| Source note | uspto-grants-1977_12 |