Methyl iodide → S-methyl-N-[2-(2-thiazolylmethylthio)ethyl]dithiocarbamate hydriodide

HRID 461514Notes

Reaction equation

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][N:10]=1.[CH3:11][I:12].[C:13](=[S:15])=[S:14]>>[IH:12].[CH3:11][S:14][C:13](=[S:15])[NH:1][CH2:2][CH2:3][S:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][N:10]=1

Participants

Reactant 3

HCID 6328Methyl iodide

HCID 6348Carbon Disulfide

HCID 129234032-[(Thiazol-2-yl)methylthio]ethylamine

Product 1

HCID 86733689S-methyl-N-[2-(2-thiazolylmethylthio)ethyl]dithiocarbamate hydriodide

Procedure

(i) 2-[(2-Aminoethyl)thiomethyl]thiazole was successively treated with carbon disulphide and methyl iodide according to the general procedure of Example 1(a) (b) to give S-methyl-N-[2-(2-thiazolylmethylthio)ethyl]dithiocarbamate hydriodide.

Sources & evidence

ORD record: ord-5d4ba0c4a8314f6ea9337fd0de6cd0d3
Source dataset: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04062967

Reaction notes

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