HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 23470325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | N,N,5,7-Tetramethyl-2,3,4,9-tetrahydro-1H-carbazol-3-amine | HCID 12361835 | — |
| Reactant | HCID 23470460 | HCID 23470460 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23470325 | HCID 23470325 | — |
Reaction Steps
Following a procedure similar to that described in Example 253 and using 10.3 g. of 3-(dimethylamino)-5,7-dimethyl-1,2,3,4-tetrahydrocarbazole (Example 221), 7.02 g. of sodium hydride, 6.65 g. of methyl iodide, and 70 ml. of dimethylformamide there was obtained 5.4 g. of 3-(dimethylamino)-5,7,9-trimethyl-1,2,3,4-tetrahydrocarbazole hydrochloride, m.p. 320°-322° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04062864 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-836febe8aa2547d3b3d71c7fa63be6d4 |
| Source note | uspto-grants-1977_12 |