HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphinodithioic acid, dicyclohexyl- → 3,5-Di-t-butyl-4-hydroxybenzyl dicyclohexylphosphinodithioate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphinodithioic acid, dicyclohexyl- | HCID 75641 | — |
| Reactant | Phenol, 4-(bromomethyl)-2,6-bis(1,1-dimethylethyl)- | HCID 612973 | — |
| Product | 3,5-Di-t-butyl-4-hydroxybenzyl dicyclohexylphosphinodithioate | HCID 21391652 | — |
Reaction Steps
3,5-di-t-butyl-4-hydroxybenzyl bromide was reacted with the ammonium salt of dicyclohexylphosphinodithioic acid to obtain 3,5-di-t-butyl-4-hydroxybenzyl dicyclohexylphosphinodithioate, m.p. 129°-131° C, which on testing lasted 475 hours* longer than the control. The total number of hours required to reach failure was 1.9 times that of the control.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064106 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-02234d352ac847228eacd63bd0fa0803 |
| Source note | uspto-grants-1977_12 |