HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 20394040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-[3-(Dimethylamino)propoxy]benzaldehyde | HCID 2995968 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20394040 | HCID 20394040 | 83.2% |
Reaction Steps
A solution of 15 g of 2-(3-dimethylaminopropoxy)benzaldehyde and 8.0 g of aniline (distilled over zinc dust) in 300 ml of ethanol is kept at room temperature for 22 hours, refluxed for 2 hours, and the solvent removed on a rotary evaporator. The residue (21.3 g) is distilled to give 17 g of an oil; boiling point 171°-175° C/0.2 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064120 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-1fbb8f56b1a64b79a9390f1b8b293076 |
| Source note | uspto-grants-1977_12 |