HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 461639Generated: October 29, 2026
1-Fluoro-2-nitrobenzene → 5-(2-Nitrophenyl)thiopyrano[3,2-b]indol-4(5H)-one
https://huagongshe.com/reaction/461639
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | Thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326608 | — |
| Product | 5-(2-Nitrophenyl)thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326622 | — |
Reaction Steps
By the same method as described in Example 7, 8.9 g of thiopyrano [3,2-b]indol-4(5H)-one is alkylated with o-fluoronitrobenzene, except the reaction is stirred for 40 hours at 95° C. The yield of product is 9.2 g, mp 207°-208° C after recrystallization from ether-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04064123 |
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| Source dataset | uspto-grants-1977_12 |
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| ORD ID | ord-944be1909e354d35bcddfbef83d23670 |
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| Source note | uspto-grants-1977_12 |
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