HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → 5-(Prop-2-yn-1-yl)thiopyrano[3,2-b]indol-4(5H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | Thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326608 | — |
| Product | 5-(Prop-2-yn-1-yl)thiopyrano[3,2-b]indol-4(5H)-one | HCID 20326612 | — |
Reaction Steps
By the same method as described in Example 7, 4.8 g of thiopyrano[3,2-b]indol-4(5H)-one is alkylated with propargyl bromide to give 5.0 g of product, mp 144° C after recrystallization from methylene chloride-ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064123 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-82e82d5e9106495ca5a52e9ade595308 |
| Source note | uspto-grants-1977_12 |