Toluene → HCID 53879595, compound

HRID 461653Notes

Reaction equation

HRID 461653 reaction equation
[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=O.[CH2:16](N)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.[C:24]1(C)C=CC=CC=1>>[CH3:1][N:2]([CH3:15])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=1[CH:9]=[CH:24][CH2:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

4

Reactant 3

HCID 1140TolueneHCID 7504BenzylamineHCID 29959682-[3-(Dimethylamino)propoxy]benzaldehyde

Product 1

HCID 53879595HCID 53879595, compound

Procedure

A solution of 20.0 g of 2-(3-dimethylaminopropoxy)-benzaldehyde and 10.3 g of benzylamine in 100 ml of toluene is heated at reflux for 1 hour in a procedure described for Example 1. The yield of product is 22.1 g, boiling point 175°-178° C/0.05 mm of Hg.

Workup

  1. temperatureat reflux for 1 hour in a procedure

Sources & evidence

ORD record
ord-688aa76015ca44e691b190c73ab56165
Source dataset
uspto-grants-1977_12
Patent number
US04064125

Reaction notes

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