反应详情

A mixture of 10.7 g. (0.065 mole) of methyl 2-ethylbenzoate, 12.5 g. (0.07 mole) of N-bromosuccinimide, 50 mg. of benzoyl peroxide, and 125 ml. of carbon tetrachloride is stirred at reflux until the reaction is complete in 2 hours. The precipitated succinimide is filtered from the cooled mixture and the filtrate is evaporated to dryness under reduced pressure leaving methyl 2-(1-bromoethyl)benzoate as the residual yellow oil in quantitative yield.

1. additionA mixture of 10.7 g
2. temperatureat reflux until the reaction
3. filtrationThe precipitated succinimide is filtered from the cooled mixture
4. customthe filtrate is evaporated to dryness under reduced pressure