Acetone → HCID 54573322, compound

HRID 461755Notes

Reaction equation

[N+]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)([O-])=O.[CH3:10][C:11]([CH3:13])=[O:12]>>[C:11]([C:13]1[CH:8]=[CH:9][CH:4]=[CH:5][C:6]=1[C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=2)[CH:5]=1)(=[O:12])[CH3:10]

Participants

Reactant 2

HCID 180Acetone

HCID 7416Nitrobenzene

Product 1

HCID 54573322HCID 54573322, compound

Procedure

Nitrobenzene is stripped with steam and the solid residue is dissolved into acetone. After filtration and the acetone evaporation, 400 g of crude product is obtained.

Workup

filtrationAfter filtration
customthe acetone evaporation

Sources & evidence

ORD record: ord-b21b75850f984fcfaf369c9be6a7f3c1
Source dataset: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04064176

Reaction notes

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