HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → 3-Tert-butyl-4-hydroxy-5-iodo-6-methylbenzylidenemalononitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-Tert-butyl-4-hydroxy-5-iodo-6-methylbenzaldehyde | HCID 21392859 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | 3-Tert-butyl-4-hydroxy-5-iodo-6-methylbenzylidenemalononitrile | HCID 53904268 | — |
Reaction Steps
In a similar manner as described in Example 2 reaction of 3-tert-butyl-4-hydroxy-5-iodo-6-methylbenzaldehyde and malononitrile gave 3-tert-butyl-4-hydroxy-5-iodo-6-methylbenzylidenemalononitrile as prisms from ethylenedichloride m.p. 158°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064266 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-88ce24beb0c64e31a6351494ec15db1a |
| Source note | uspto-grants-1977_12 |