HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 20560054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-[2-(Pyridin-2-yl)ethyl]aniline | HCID 4715422 | — |
| Reactant | HCID 20560024 | HCID 20560024 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 20560054 | HCID 20560054 | — |
Reaction Steps
Reaction of 2-(o-aminophenethyl)-5-ethylpyridine with acetic anhydride and formic acid according to the procedure described in Example 2 (b) for 2-(o-aminophenethyl)pyridine provides the formylated product 5-ethyl-2-(o-formamidophenethyl)pyridine which can be crystallized from isopropyl ether, m.p. 62°-63.5° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064254 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-7aae3238e3274839b41ea09233469e79 |
| Source note | uspto-grants-1977_12 |