HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → N-{2-[2-(1-Ethylpiperidin-2-yl)ethyl]phenyl}-4-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 2-[2-(1-Ethylpiperidin-2-yl)ethyl]aniline | HCID 20559983 | — |
| Product | N-{2-[2-(1-Ethylpiperidin-2-yl)ethyl]phenyl}-4-methoxybenzamide | HCID 20559999 | — |
Reaction Steps
Reaction of 2-(2-aminophenethyl)-1-ethylpiperidine with anisoyl chloride according to the procudure of Example 25 provides 2'-[2-(1-ethyl-2-piperidyl)ethyl]-p-anisanilide, m.p. 136.5°-137.5° C. (corr.), from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064254 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-af7815bd13754f8eb15825284b497312 |
| Source note | uspto-grants-1977_12 |