HuagongsheHuagongshe Chemistry Print Report · For research reference only
2'-(2-Pyridylmethyl)-p-anisanilide → 2'-(2-Piperidylmethyl)-p-anisanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2'-(2-Pyridylmethyl)-p-anisanilide | HCID 20559990 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2'-(2-Piperidylmethyl)-p-anisanilide | HCID 20560093 | — |
Reaction Steps
Reduction of 2'-(2-pyridylmethyl)-p-anisanilide (4.65 g., 0.0146 mole) according to the procedure of Walker, J. Org. Chem., 27, 2966 (1962), in 150 ml. of acetic acid with 2.35 g. of 10% palladium on carbon catalyst affords 2'-(2-piperidylmethyl)-p-anisanilide, m.p. 108°-109° C. (corr.), from benzene-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064254 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-4e17676155a54dcb952666af101fd4c1 |
| Source note | uspto-grants-1977_12 |