HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → 2-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | (2-Chloroethyl)phosphonic dichloride | HCID 69645 | — |
| Reactant | 2-chloroethanephosphonic acid N-monoisopropylamide chloride | HCID 86735308 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-chloroethanephosphonic acid isopropyl ester N-monoisopropylamide | HCID 86735309 | — |
Reaction Steps
The 2-chloroethane-phosphonic acid N-mono-isopropylamide chloride used as starting product was prepared from 2-chloroethane-phosphonic acid dichloride and iso-propylamine in toluene at 0° C. Yield: 91% of the theory, nD28 = 1.4854.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065288 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-6d8821fac516425287dcfb50e1433db5 |
| Source note | uspto-grants-1977_12 |