2-Methyl-8-hydroxyquinoline → HCID 4670724, compound

HRID 462041Notes

Reaction equation

HRID 462041 reaction equation
CC1C=CC2C(=C(O)C=CC=2)N=1.[CH3:13][C:14]1[CH:23]=[CH:22][C:21]2[C:16](=[C:17]([OH:36])[C:18]([CH:24]=[CH:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35])=[CH:19][CH:20]=2)[N:15]=1>>[CH3:13][C:14]1[CH:23]=[CH:22][C:21]2[C:16](=[C:17]([OH:36])[C:18]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH3:35])=[CH:19][CH:20]=2)[N:15]=1

Participants

3

Reactant 2

HCID 132242-Methyl-8-hydroxyquinolineHCID 70634289HCID 70634289, compound

Product 1

HCID 4670724HCID 4670724, compound

Procedure

Example I was essentially repeated using 2-methyl-8-hydroxyquinoline in place of 5-chloro-8-hydroxyquinoline. The resultant 2-methyl-7-dodecenyl-8-hydroxyquinoline was hydrogenated by the procedure of Example II, Part B to give 2-methyl-7-dodecyl-8-hydroxyquinoline.

Sources & evidence

ORD record
ord-0a70967f87274cc3b16d44279d6b7392
Source dataset
uspto-grants-1977_12
Patent number
US04065455

Reaction notes

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