HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-nitrobenzoic acid → 2-Methyl-3-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-nitrobenzoic acid | HCID 16096 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2-Methyl-3-nitrobenzoyl chloride | HCID 12194872 | 95% |
Reaction Steps
A mixture of 2-methyl-3-nitrobenzoic acid (9.2 grams; 0.05 mole) and 15 mls. of thionyl chloride was heated at reflux for 6 hours. The excess thionyl chloride was removed by distillation to obtain 2-methyl-3-nitrobenzoyl chloride (9.5 grams; 95% yield; m.p. 68°-70° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065477 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-51978b0a2f0b4013b24dcf8634f94559 |
| Source note | uspto-grants-1977_12 |