2-Methyl-3-nitrobenzoic acid → 2-Methyl-3-nitrobenzoyl chloride

HRID 462092Notes

Reaction equation

[CH3:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].S(Cl)([Cl:16])=O>>[CH3:1][C:2]1[C:10]([N+:11]([O-:13])=[O:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([Cl:16])=[O:5]

Participants

Reactant 2

HCID 160962-Methyl-3-nitrobenzoic acid

HCID 24386Thionyl Chloride

Product 1

HCID 121948722-Methyl-3-nitrobenzoyl chloride

Procedure

reacting said 2-methyl-3-nitrobenzoic acid in refluxing thionyl chloride to form 2-methyl-3-nitrobenzoyl chloride,

Sources & evidence

ORD record: ord-db4f3e07dd8d4748abce5cb8924d8eda
Source dataset: uspto-grants-1977_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04065477

Reaction notes

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