Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Chloromethyl)-1-methoxy-4-nitrobenzene → N-methyl-N-(5-nitro-2-methoxybenzyl)N,N-bis(3-formamidopropyl)ammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Chloromethyl)-1-methoxy-4-nitrobenzene | HCID 2529377 | — |
| 반응물 | Formamide, N,N'-[(methylimino)di-3,1-propanediyl]bis- | HCID 3084810 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-methyl-N-(5-nitro-2-methoxybenzyl)N,N-bis(3-formamidopropyl)ammonium chloride | HCID 20336842 | — |
반응 단계
Proceeding in a manner similar to that described above in B-8a, 142 parts of N,N-bis(3-formamidopropyl)methylamine and 141 parts of 5-nitro-2-methoxybenzyl chloride were interacted in 115 parts of water to obtain N-methyl-N-(5-nitro-2-methoxybenzyl)-N,N-bis(3-formamidopropyl)ammonium chloride. The product was not isolated but was used directly in solution for reduction of the nitro group.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04065500 |
| 출처 데이터셋 | uspto-grants-1977_12 |
| ORD ID | ord-5b9778496e57456e8370216627ce7be9 |
| 출처 메모 | uspto-grants-1977_12 |