化工社化工社 化学情報印刷レポート · 研究参考用
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 反応物 | 2-chloro-N-(2-methoxy-5-nitrophenyl)acetamide | HCID 2362603 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733013 | — |
反応手順
In a manner similar to that described above in B-1a, and using 27.3 parts of N-(3-dimethylaminopropyl)formamide, 48 parts of 2-chloro-2'-methoxy-5'-nitroacetanilide, and 157 parts of isopropyl alcohol there was obtained 52.6 parts of N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid, m.p. 86°-88°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04065500 |
| 出典データセット | uspto-grants-1977_12 |
| ORD ID | ord-be147f3e19b641a9837d46e8cfee54c9 |
| 出典メモ | uspto-grants-1977_12 |